Abstract
The main goal of the research was to employ the unique data delivered by various methods to improve the determination of rock reservoir properties. Results of X-ray computed tomography (XRCMT), one of the newest techniques providing high-resolution images of rocks, were used to show that very precise information from this tool is complementary to results from other methods. Standard laboratory measurements (helium pycnometer, mercury injection porosimetry, permeameter) and sophisticated experiments (X-ray computed tomography and nuclear magnetic resonance spectroscopy) were performed to obtain and compare results. Four types of specimens: typical Miocene sandstone-mudstone-claystone rock samples, artificial corundum specimens, shale gas plugs, and limestone sample were investigated to obtain the porosity, permeability, density, and other parameters used in rock descriptions. Mutual relationships between selected groups of rock material properties were presented to provide an integral picture of rock characteristics. The XRCMT results were in general not influenced by lithology, but there were observed shaliness effects on the shape of pores, cross sections, and the tortuosity of porous channels. An analysis of the average porosity and the standard deviation of each XRCMT plot provided information about differences in the heterogeneity of a formation. Thus, the XRCMT method was recommended in pore space parameter determination for microfracture fluid propagation monitoring. There was also observed equivalence between part of the NMR signal from clay-bound water and the XRCMT volume subgroups in porosity/permeability—structural classes I and II. So, the use of the two-subsample approach in the XRCMT interpretation was promoted.
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References
Nolen-Hoeksema, R.: Flow through pores. Oilfield Rev. Autumn. 2014, 63–64 (2014)
TerraTek: Tight rock analysis—permeability. Project nr 20810033, Dec. 22, Report of the TerraTek Schlumberger Reservoir Laboratory. Archive of Department of Geophysics, FGGEP AGH UST, Krakow, Poland (2014)
Firouzi, M., Alnoaimi, K., Kovscek, A., Wilcox, J.: Klinkenberg effect on predicting and measuring helium permeability in gas shales. Int. J. of Coal Geol. 123, 62–68 (2014)
Jarzyna, J.A., Bała M.J., Mortimer, Z.M., Puskarczyk, E.: Reservoir parameter classification of a Miocene formation using a fractal approach to well logging, porosimetry and nuclear magnetic resonance. Geophys. Prospect. 61, 1006–1021 (2013a)
Such, P.: Przestrzeń porowa skał łupkowych. Nafta-Gaz 9, 561–565 (2012)
Zinovik, I., Poulikakos, D.: On the permeability of fractal tube bundles. Transp. Porous Media 94(3), 747–757 (2012)
Peveraro, R., Thomas, E.C.: Effective porosity: a defensible definition for shaly sands. SPWLA 51 st Annual Logging Symposium, June 19–23 (2010)
Leśniak, G., Such, P.: Fractal approach. Analysis of images and diagenesis in pore space evaluation. Nat. Resour. Res. 14(4), 317–324 (2005)
Krakowska, P.I., Madejski, P., Jarzyna, J.: Permeability estimation using CFD modeling in tight Carboniferous sandstone. In: Proceedings of 76th EAGE Conference and Exhibition 2014, 16-19 June, EAGE EarthDoc Database. ISSN 2214-4609, Th P06 05, pp 1–5 (2014)
Beard, D.C., Weyl, P.K.: Influence of texture on porosity and permeability of unconsolidated sand. AAPG Bull. 57(2), 349–369 (1973)
Gingras, M.K., Pemberton, S.G., Smith, M.: Bioturbation: reworking sediments for better and worse. Oilfield Review Winter 2015(/15), 46–60 (2014)
Aplin, A.C., Macquaker, J.H.S.: Mudstone diversity: origin and implications for source, seal and reservoir properties of petroleum system. AAPG Bull. 95(12), 2031–2059 (2011)
Nadeev, A., Mikhailov, D., Chuvilin, E., Koroteev, D., Shako, V.: Visualization of clay and frozen substances inside porous rocks using X-ray micro-computed tomography. Micros. Anal. – Tomogr. Suppl. 27(2), 8–11 (2013)
Mutina, A., Bruyndonckx, P.: Combined micro-X-ray tomography and micro-X-ray fluorescence study of reservoir rocks: applicability to core analysis. Microsc. Anal. – Compos. Anal. Suppl. 27(4), 4–6 (2013)
Dohnalik, M.: Improving the ability of determining reservoir rocks parameters using X-ray computed microtomography. Ph.D. Thesis, AGH University of Science and Technology in Krakow. Main Library (2013)
Karpyn, Z., Alakmi, A., Parada, C., Grader, A.S., Halleck, P.M., Karacan, O.: Mapping fracture apertures using micro computed tomography. In: International Symposium of the Society of the Core Analysts, 21-24 September, Pau, France, SCA 2003–50 (2003)
Madonna, C., Almqvist, B., Seanger, E.: Digital rock physics: numerical prediction of pressure-dependent ultrasonic velocities using micro-CT imaging. Geophys. J. Int. 189, 1475–1482 (2012)
Josh, M., Esteban, L., Delle Piane, C., Sarout, J., Dewhurst, D.N., Clennell, M.B.: Laboratory characterization of shale properties. J. Petrol. Sci. and Eng. 88–89, 107–124 (2012)
Vavra, C.L., Kaldi, J.G., Sneider, R.M.: Geological applications of capillary pressure: a review (1). AAPG Bull. 76(6), 840–850 (1992)
Xiao, L., Mao, Z.Q., Xiao, Z.X., Zhang, C.: A new method to evaluate reservoir pore structure consecutively using NMR and capillary pressure data. SPWLA 49th Annual Logging Symposium 2008, paper AA (2008)
Xiao, L., Mao, Z.Q., Wang, Z.N, Yin, Y., Liu, X.G, Xie, B.: Tight gas sands permeability estimation from nuclear magnetic resonance (NMR) logs and mercury injection capillary pressure (MICP) data. Acta Geophys., accepted after reviews (2013)
Mohammadlou, M.H., Mork, M.B.: Integrated petrophysical analysis in tight and brecciated carbonate reservoir. Proceedings of the SPE Annual Technical Conference and Exhibition, Florence, Italy, 19-22 September (2010)
Jarzyna, J.A., Krakowska, P.I., Puskarczyk, E., Semyrka, R.: Rock reservoir properties from the comprehensive interpretation of nuclear magnetic resonance and mercury injection porosimetry laboratory results. Appl. Magn. Reson. 46, 95–115 (2015)
Bielecki, J., BoŻek, S., Lekki, J., Stachura, Z., Kwiatek, W.M.: Applications of the Cracow X-ray microprobe in tomography. Acta Phys. Pol. A 115(2), 537–541 (2009)
Jarzyna, J., Wawrzyniak-Guz, K., Puskarczyk, E., Krakowska, P., Bała, M., Niepsuj, M., Marzec, P., Pietsch, K., Gruszczyk, M. (eds.): Spatial distribution of petrophysical parameters on the basis of laboratory investigations, well logging and seismics, GOLDRUK, Kraków (2013b)
Bielecki, J.: Investigations of complex structures by means of the computed microtomography method. Ph.D, Thesis, Library of the Institute of Nuclear Physics Polish Academy of Sciences (2011)
Chang, D., Vinegar, H.V., Morris, C., Straley, C.: Effective porosity, producible fluid in carbonates from NMR logging. SPWLA 35th Annual Logging Symposium 1994, paper A (1994)
Puskarczyk, E., Jarzyna, J., Kwiatek, W.M., Tkocz, K.: Standard model of rock based on laboratory tests for artificial samples, vol. 198 (2014)
Jarzyna, J., Bała, M., Golonka, J., Grabowska, T., Lemberger, M., Pietsch, K., Stefaniuk, M.: New aspects of geophysical measurements interpretation to verify possibility of hydrocarbon prospection in Western Carpathians. Report of the scientific grant MNiI, nr 4T12B 025 28, archive of the Department of Geophysics AGH UST (2005)
Jarzyna, J., Puskarczyk, E., Wójcik, A., Semyrka, R.: NMR and mercury porosimetry measurements for the selected rock samples of the Western Carpathians. Geol. 33 4(/1), 211–236 (2007)
Krakowska, P.: Reservoir potential of the Precambrian and Paleozoic sedimentary rocks on the basis of laboratory measurements and well logging. Ph.D. Thesis, AGH University of Science and Technology in Krakow, Main Library (2014)
Porėbski, S., Prugar, W., Zacharski, J.: Silurian shales of the East European Platform in Poland—some exploration problems. Geol. Rev. 61(/11), 630–638 (2013)
Kaczmarczyk, J., Dohnalik, M., Cnude, V., Zalewska, J.: The interpretation of X-ray computed microtomography images of rocks as an application of volume image processing and analysis. Proceedings of 18th WSCG International Conference on Computer Graphics, Visualization and Computer Vision, Pilznen, Czech Republic, University of West Bohemia, ISBN 978-80-86943-87-9, 23–30 (2010)
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Jarzyna, J.A., Krakowska, P.I., Puskarczyk, E. et al. X-ray computed microtomography—a useful tool for petrophysical properties determination. Comput Geosci 20, 1155–1167 (2016). https://doi.org/10.1007/s10596-016-9582-3
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DOI: https://doi.org/10.1007/s10596-016-9582-3