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Table 5 Variation of impurity concentrations during the precipitation step

From: Identification of uranium signatures relevant for nuclear safeguards and forensics

 

Ratio precipitate versus loaded solution (separation factor)

Barren mother concentrations in (μg g−1) (±uncertainty)

 

Ratio precipitate versus loaded solution (separation factor)

Barren mother concentrations in μg g−1 (±uncertainty)

Ag

 

Less than 3.9E−02

Na

4.43

1.22E+01 ± 7.1E−01

Al

0.039

Less than 9.5E−01

Nb

0.82

Less than 9.8E−04

As

1.51

3.38E−02 ± 2.0E−03

Nd

0.23

Less than 1.4E−03

Au

Higher than 186

1.06E−02 ± 6.2E−04

Ni

 

Less than 8.5E−02

B

1.50

8.08E−01 ± 4.7E−02

Os

 

Less than 5.3E−02

Ba

0.34

Less than 4.6E−03

P

1.05

Less than 2.3E+00

Be

 

Less than 5.1E−02

Pb

 

Less than 2.0E−02

Bi

1.89

5.20E−03 ± 3.0E−04

Pd

Higher than 3

1.16E−03 ± 6.7E−05

Ca

1.41

9.52E+00 ± 5.5E−01

Pr

 

Less than 9.0E−05

Cd

0.95

Less than 1.2E−03

Pt

1.16

Less than 8.1E−04

Ce

0.11

Less than 3.3E−04

Rb

1.10

Less than 2.4E−02

Co

166

1.04E+00 ± 6.0E−02

Re

7.85

2.89E−04 ± 1.7E−05

Cr

0.39

Less than 6.7E−03

Ru

 

Less than 4.4E−04

Cs

 

Less than 5.9E−03

S

114

1.46E+04 ± 8.5E+02

Cu

 

Less than 4.0E−02

Sb

0.81

Less than 5.0E−04

Dy

0.70

Less than 1.1E−04

Sc

0.86

Less than 1.4E−03

Er

 

Less than 9.6E−05

Se

Higher than 12

2.64E−01 ± 1.5E−02

Eu

 

Less than1.1E−04

Si

 

Less than 6.5E+01

Fe

0.28

Less than 3.9E−01

Sm

 

Less than 7.0E−04

Ga

0.62

Less than 2.5E−03

Sn

Higher than 78

Less than 1.7E−02

Gd

0.36

Less than 2.5E−04

Sr

0.32

9.57E−04 ± 5.5E−05

Ge

Higher than 1.4

Less than 1.0E−01

Ta

 

Less than 3.7E−03

Hf

0.96

Less than 2.1E−04

Tb

 

Less than 4.1E−05

Hg

 

Less than 3.2E−02

Te

1.15

Less than 5.1E−03

Ho

 

Less than 2.9E−05

Th

0.84

Less than 6.1E−04

In

 

Less than 1.0E−03

Ti

0.54

Less than 1.3E−02

Ir

1.29

Less than 8.5E−03

Tl

 

Less than 5.0E−04

K

1.82

1.87E+00 ± 1.1E−01

Tm

 

Less than 3.7E−05

La

0.81

Less than 5.0E−04

V

 

Less than 8.3E−03

Li

Higher than 1.8

Less than6.3E−02

W

0.92

Less than 3.3E−03

Lu

 

Less than 2.7E−05

Y

0.32

Less than 7.2E−04

Mg

3.57

4.88E+00 ± 2.8E−01

Yb

 

Less than 5.8E−05

Mn

14.2

7.72E−01 ± 4.5E−02

Zn

1.41

Less than 4.8E−01

Mo

1.13

1.14E−03 ± 6.6E−05

Zr

0.83

5.49E−03 ± 3.2E−04

  1. Concentration ratios in the precipitate (ADU slurry-1) relative to that of in the loaded solution (separation factor)
  2. Barren mother concentration results in microgram analyte per gram U in the sample are also indicated. Separation factors higher than 1.25, less than 0.75 and between 0.75 and 1.25 are highlighted